反応式
[CH3:1][N:2]([CH3:13])[C:3]1[CH:8]=[CH:7][C:6]([CH2:9][C:10]([OH:12])=O)=[CH:5][CH:4]=1.[F:14][C:15]([F:25])([F:24])[S:16][C:17]1[CH:23]=[CH:22][C:20]([NH2:21])=[CH:19][CH:18]=1>>[CH3:13][N:2]([CH3:1])[C:3]1[CH:4]=[CH:5][C:6]([CH2:9][C:10]([NH:21][C:20]2[CH:22]=[CH:23][C:17]([S:16][C:15]([F:25])([F:14])[F:24])=[CH:18][CH:19]=2)=[O:12])=[CH:7][CH:8]=1参加物
3
実験手順
The product was prepared from 2-(4-(dimethylamino)phenyl)acetic acid (23 mg) and 4-trifluoromethylthioaniline (28 mg) according to Method C: 1H NMR (300 MHz, CDCl3) δ ppm 2.98 (s, 6H), 3.66 (s, 2H), 6.72-6.78 (m, 2H), 7.14-7.19 (m, 2H), 7.19 (s, 1H), 7.43-7.51 (m, 2H), 7.52-7.57 (m, 2H); MS (ESI-pos) m/z 355.0 (M+H)+.
出典と根拠
- ORDレコード
- ord-c3ba8f93e3fb4d70827d005bd4d2b2ef
- 出典データセット
- uspto-grants-2011_08
- 特許番号
- US07994223B2
関連ノート
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