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Vinyl Acetate → HCID 178525781、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Vinyl Acetate | HCID 7904 | — |
| 反応物 | 4-Hydroxycyclohexyl benzoate | HCID 238109 | — |
| 溶媒 | Diisopropyl Ether | HCID 7914 | — |
| 生成物 | HCID 178525781 | HCID 178525781 | 46% |
反応手順
To a solution of 4-hydroxycyclohexyl benzoate (81.5 g) and Lipase QLG (40 g) in diisopropyl ether (800 mL) was added vinyl acetate (120 mL) at room temperature. After being stirred at room temperature for 2 hr, Lipase QLG was filtered off. The filtrate was concentrated under reduced pressure. The residue was purified by silica gel column chromatography to give the title compound as a colorless solid (37.5 g, 46%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07998968B2 |
| 出典データセット | uspto-grants-2011_08 |
| ORD ID | ord-9452e169fac44bedba91133d72773432 |
| 出典メモ | uspto-grants-2011_08 |