3-Nitro-4-(trifluoromethoxy)benzoic acid → 3-Amino-4-(trifluoromethoxy)benzoic acid
反応式
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[O:13][C:14]([F:17])([F:16])[F:15])[C:7]([OH:9])=[O:8])([O-])=O>CO>[NH2:1][C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[O:13][C:14]([F:15])([F:16])[F:17])[C:7]([OH:9])=[O:8]参加物
3
実験手順
A solution of 3-nitro-4-trifluoromethoxybenzoic acid (3 g) in methanol (240 ml) was hydrogenated at 50° C. and 50 bar using H-cube apparatus. The methanol solution was evaporated giving the title compound as a white solid (2.58 g).
後処理
- customwas hydrogenated at 50° C.
- customThe methanol solution was evaporated
出典と根拠
- ORDレコード
- ord-ebfd23b88677408e80c4208b95b8ebd6
- 出典データセット
- uspto-grants-2011_08
- 特許番号
- US08008303B2
反応ノート
読み込み中…