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Acetone → 5-Benzyloxy-2,2-dimethyl-1,3-dioxane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetone | HCID 180 | — |
| 反応物 | 2-(Phenylmethoxy)-1,3-propanediol | HCID 203567 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 5-Benzyloxy-2,2-dimethyl-1,3-dioxane | HCID 20364889 | — |
反応手順
Using the procedure of Example 51, 2-benzyloxy-1,3-propanediol and acetone were reacted, using benzene as solvent, to give, after distillation using a short path column, 5-benzyloxy-2,2-dimethyl-1,3-dioxane. The nmr spectrum was consistent with the assigned structure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04077982 |
| 出典データセット | uspto-grants-1978_03 |
| ORD ID | ord-80f56de90df74adaade2cd08e85c9ee3 |
| 出典メモ | uspto-grants-1978_03 |