Diglyme → HCID 178420510、化合物

HRID 1679040

反応式

HRID 1679040 の反応式
C([N:7]1[C:11]2[N:12]=[CH:13][C:14]3[C:15]([O:23][C:24]4[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=4)=[N:16][C:17]4[N:18]([N:20]=[CH:21][N:22]=4)[C:19]=3[C:10]=2[CH:9]=[N:8]1)C1OC=CC=1.COCCOCCOC.[Se](=O)=O>>[C:24]1([O:23][C:15]2[C:14]3[CH:13]=[N:12][C:11]4[NH:7][N:8]=[CH:9][C:10]=4[C:19]=3[N:18]3[N:20]=[CH:21][N:22]=[C:17]3[N:16]=2)[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=1

参加物

4

反応物 3

HCID 8150DiglymeHCID 24007Selenium DioxideHCID 227585308-furfuryl-5-phenyloxy-8H-pyrazolo[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]pyrimidine

生成物 1

HCID 178420510HCID 178420510、化合物

実験手順

0.01 mol. of 8-furfuryl-5-phenyloxy-8H-pyrazolo[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]pyrimidine is heated in 50 ml. of diethyleneglycol dimethyl ether containing 0.01 mol. of selenium dioxide at reflux temperature with stirring for two hours. The mixture is filtered hot and evaporated to dryness. 5-Phenyloxy-8H-pyrazolo[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]pyrimidine remains.

後処理

  1. filtrationThe mixture is filtered hot
  2. customevaporated to dryness

出典と根拠

ORDレコード
ord-5bacc5ef9b764caaa57482a79a0efa92
出典データセット
uspto-grants-1978_03
特許番号
US04078064

関連ノート

読み込み中…