1,3,5-Triazinane-2,4-dione, 1,3,5-trimethyl- → HCID 70575974、化合物

HRID 1679495ノート

反応式

HRID 1679495 の反応式
[Cl:1]N1C(=O)NC(=O)N(Cl)C1=O.[Na].[O:13]=[C:14]1[N:19]([CH3:20])[C:18](=[O:21])[N:17]([CH3:22])[CH2:16][N:15]1[CH3:23]>CO>[Cl-:1].[O:13]=[C:14]1[N:19]([CH3:20])[C:18](=[O:21])[N:17]([CH3:22])[CH2:16][NH+:15]1[CH3:23]

参加物

4

反応物 2

HCID 1816881,3,5-Triazinane-2,4-dione, 1,3,5-trimethyl-HCID 86657659Sodium dichlorocyanuric acid

生成物 1

HCID 70575974HCID 70575974、化合物

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

17.8 g (0.1 mol) of sodium dichlorocyanuric acid are added to 15.7 g (0.1 mol) of 2,4-dioxo-hexahydro-1,3,5-trimethyl-s-triazine in 50 ml of methanol and the mixture is stirred. The cyanuric acid which has precipitated is then filtered off and the filtrate is evaporated. The residue which remains on evaporation is digested with water. After renewed filtration to remove residual cyanuric acid, an aqueous solution of the same compound as in Example g is obtained.

後処理

  1. customThe cyanuric acid which has precipitated
  2. filtrationis then filtered off
  3. customthe filtrate is evaporated
  4. customThe residue which remains on evaporation
  5. filtrationfiltration
  6. customto remove residual cyanuric acid
  7. customan aqueous solution of the same compound as in Example g is obtained

出典と根拠

ORDレコード
ord-3769b7e41fcb49179062e8fdcf5f8766
出典データセット
uspto-grants-1978_03
特許番号
US04080502

反応ノート

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