Hydrochloric Acid → HCID 12824993、化合物

HRID 1679508ノート

反応式

HRID 1679508 の反応式
[Cl:1][CH:2]([CH2:6][C:7]1[CH:12]=[CH:11][C:10]([O:13][CH2:14][C:15]([CH3:23])([CH3:22])[C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[CH:9][CH:8]=1)[C:3]([O-:5])=[O:4].[Na+].Cl>O>[Cl:1][CH:2]([CH2:6][C:7]1[CH:12]=[CH:11][C:10]([O:13][CH2:14][C:15]([CH3:23])([CH3:22])[C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[CH:9][CH:8]=1)[C:3]([OH:5])=[O:4]

参加物

4

反応物 2

HCID 313Hydrochloric AcidHCID 23695280HCID 23695280、化合物

生成物 1

HCID 12824993HCID 12824993、化合物収率 91.4%

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

In 5 ml of water is dissolved 350 mg of sodium 2-chloro-3-[4-(2,2-dimethyl-2-phenylethyloxy)phenyl]propionate, followed by the addition of 2-N hydrochloric acid. The oily substance separated out is extracted with ether. The extract is washed with water and the solvent is distilled off. The described procedure gives 300 mg of 2-chloro-3-[4-(2,2-dimethyl-2-phenylethyloxy)phenyl]propionic acid, as a yellow oily substance.

後処理

  1. customThe oily substance separated out
  2. extractionis extracted with ether
  3. washThe extract is washed with water
  4. distillationthe solvent is distilled off

出典と根拠

ORDレコード
ord-bc91a5d96a9d417b8328ab8e47035566
出典データセット
uspto-grants-1978_03
特許番号
US04080505

反応ノート

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