Ethanol → Ethyl 2-(2,3-dichlorophenoxy)acetimidate hydrochloride
反応式
[Cl:1][C:2]1[C:11]([Cl:12])=[CH:10][CH:9]=[CH:8][C:3]=1[O:4][CH2:5][C:6]#[N:7].[CH2:13]([OH:15])[CH3:14]>CCOCC>[ClH:1].[Cl:1][C:2]1[C:11]([Cl:12])=[CH:10][CH:9]=[CH:8][C:3]=1[O:4][CH2:5][C:6](=[NH:7])[O:15][CH2:13][CH3:14]参加物
4
実験手順
Obtained using the procedure described in section a of Example 6, starting with 219.8 g (1.086 moles) of (2,3-dichlorophenoxy)acetonitrile [prepared according to R. W. Fuller et al., J. Am. Chem. Soc. 1973, 16, 101] and 50.0 g (1.086 moles) of absolute ethanol in 1750 ml of ether. Reaction time: 16 hours at 0° C. Yld: 293.5 g (95%), m.p. 167°-169° C.
後処理
- customObtained
- customReaction time
- custom16 hours
- customat 0° C
出典と根拠
- ORDレコード
- ord-730e8c66f90c4ce8b626f565aa5e5822
- 出典データセット
- uspto-grants-1992_12
- 特許番号
- US05167949
反応ノート
読み込み中…