関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | 4-Amino-2-(benzyloxymethyl)pteridine | HCID 10778229 | — |
| 溶媒 | Sodium Hydroxide | HCID 14798 | — |
| 生成物 | 2-Benzyloxymethyl-4(3H)-pteridinone | HCID 135461697 | — |
反応手順
Obtained using the procedure described in section b of Example 9, starting with 10.0 g (0.037 mole) of crude 4-amino-2-(benzyloxymethyl)pteridine in 300 ml of 5% aqueous sodium hydroxide. Heating time, 2 hours at 80° C. Yld: 8.2 g (83%), m.p. 157°-159° C. (ethanol).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05167949 |
|---|
| 出典データセット | uspto-grants-1992_12 |
|---|
| ORD ID | ord-82026c598473433ca2da58396cb7ae37 |
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| 出典メモ | uspto-grants-1992_12 |
|---|
