[2-(Pyridin-2-yl)-1,3-thiazol-4-yl]methanol → 2-(Pyridin-2-yl)-1,3-thiazole-4-carbaldehyde
反応式
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]1[S:8][CH:9]=[C:10]([CH2:12][OH:13])[N:11]=1>C1(C)C=CC=CC=1.[O-2].[Mn+2]>[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]1[S:8][CH:9]=[C:10]([CH:12]=[O:13])[N:11]=1参加物
4
実験手順
5.8 g of the product of Stage D in 60 ml of toluene were refluxed for 2 hours in the presence of 13 g of manganese oxide and filtration was carried out. The solvent was evaporated under reduced pressure to obtain 5 g of the expected product melting at 131° C.
後処理
- customThe solvent was evaporated under reduced pressure
出典と根拠
- ORDレコード
- ord-1199fb9f238f42b4b478dfad89ac424b
- 出典データセット
- uspto-grants-1997_06
- 特許番号
- US05635485
反応ノート
読み込み中…