Dimethylamine → 4-[5-(5-Dimethylaminomethyl-thiophen-2-yl)-[1,2,4]oxadiazol-3-yl]-2,6-dimethyl-phenol
反応式
[OH:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([C:9]2[N:13]=[C:12]([C:14]3[S:18][C:17]([CH:19]=O)=[CH:16][CH:15]=3)[O:11][N:10]=2)=[CH:4][C:3]=1[CH3:21].[CH3:22][NH:23][CH3:24]>>[CH3:22][N:23]([CH2:19][C:17]1[S:18][C:14]([C:12]2[O:11][N:10]=[C:9]([C:5]3[CH:6]=[C:7]([CH3:8])[C:2]([OH:1])=[C:3]([CH3:21])[CH:4]=3)[N:13]=2)=[CH:15][CH:16]=1)[CH3:24]参加物
3
実験手順
The title compound is prepared from 5-[3-(4-hydroxy-3,5-dimethyl-phenyl)-[1,2,4]oxadiazol-5-yl]-thiophene-2-carbaldehyde and dimethylamine according to Method B; LC-MS: tR=0.75 min; [M+1]+=330.05.
出典と根拠
- ORDレコード
- ord-19f93626b9504d32b37196e1a64ed35b
- 出典データセット
- uspto-grants-2012_04
- 特許番号
- US08148410B2
反応ノート
読み込み中…