2-Ethyl-3-methoxyaniline → HCID 178437263、化合物

反応式

[CH2:1]([C:3]1[C:10]([NH2:11])=[CH:9][CH:8]=[CH:7][C:4]=1[O:5][CH3:6])[CH3:2].[OH:12][C:13]1C2C(=C(C)C(OC)=CC=2)N=[C:15]([C:26]2[S:27][CH:28]=[C:29]([CH:31]([CH3:33])[CH3:32])[N:30]=2)[CH:14]=1>>[CH2:1]([C:3]1[C:4]([O:5][CH3:6])=[CH:7][CH:8]=[C:9]2[C:10]=1[N:11]=[C:15]([C:26]1[S:27][CH:28]=[C:29]([CH:31]([CH3:32])[CH3:33])[N:30]=1)[CH:14]=[C:13]2[OH:12])[CH3:2]

参加物

反応物 2

HCID 141128132-Ethyl-3-methoxyaniline

HCID 1784876922-(4-Isopropylthiazol-2-YL)-7-methoxy-8-methylquinolin-4-OL

生成物 1

HCID 178437263HCID 178437263、化合物

実験手順

The title compound was prepared from 2-ethyl-m-anisidine (68) following the procedure (Steps 3-5) reported for the preparation of 4-hydroxy-2-(4-isopropylthiazole-2-yl)-7-methoxy-8-methylquinoline (36): m/z=329 (M+H)+.

出典と根拠

ORDレコード: ord-af30853828eb4938a1eaa3c397030d66
出典データセット: uspto-grants-2012_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08148399B2

反応ノート

読み込み中…