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4-Methoxy-5-nitro-2-(pyrrolidin-1-yl)pyridine → 4-Methoxy-2-(pyrrolidin-1-yl)-5-aminopyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methoxy-5-nitro-2-(pyrrolidin-1-yl)pyridine | HCID 57431518 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 生成物 | 4-Methoxy-2-(pyrrolidin-1-yl)-5-aminopyridine | HCID 57431519 | 96.3% |
反応手順
The method described in Stage 12.2 is followed, starting from 1.5 g (6.72 mmol) of 4-methoxy-5-nitro-2-(pyrrolidin-1-yl)-pyridine, obtained in Stage 6.1, and 0.15 g of palladium on charcoal at 10%. We thus obtain 1.25 g of the expected product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08153650B2 |
| 出典データセット | uspto-grants-2012_04 |
| ORD ID | ord-d935616ab5d747efb0b68f8cc018e8c7 |
| 出典メモ | uspto-grants-2012_04 |