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2,6-Xylyl isocyanate → 1-Cyclohexyl-3-(2,6-dimethyl-phenyl)-1-(2-phenyl-2H-indazol-3-yl)-urea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Xylyl isocyanate | HCID 98787 | — |
| 反応物 | N-Cyclohexyl-2-phenyl-2H-indazol-3-amine | HCID 12318206 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 1-Cyclohexyl-3-(2,6-dimethyl-phenyl)-1-(2-phenyl-2H-indazol-3-yl)-urea | HCID 45110617 | — |
反応手順
In analogy to the procedure described in example 1.2, cyclohexyl-(2-phenyl-2H-indazol-3-yl)-amine (example 1.1) was reacted with 2-isocyanato-1,3-dimethyl-benzene ([28556-81-2]) in toluene for 72 h under reflux conditions to give the title compound as yellow oil. MS: m/e=439.3 [M+H+].
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08153663B2 |
| 出典データセット | uspto-grants-2012_04 |
| ORD ID | ord-a03121c44e3149f7b2a0a96fa6ca83bd |
| 出典メモ | uspto-grants-2012_04 |