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Dimethylamine → 5-(Dimethylamino)-2-nitrobenzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylamine | HCID 674 | — |
| 反応物 | 5-Chloro-2-nitrobenzoic acid | HCID 17286 | — |
| 生成物 | 5-(Dimethylamino)-2-nitrobenzoic acid | HCID 12715793 | — |
反応手順
Concretely, 5-chloro-2-nitrobenzoic acid is dissolved in a dimethylamine aqueous solution and heated to produce 5-dimethylamino-2-nitrobenzoic acid. Hydrochloric acid is added to the reaction solution to precipitate out the product as a solid material. The solid material is separated to obtain 5-dimethylamno-2-nitrobenzoic acid almost quantitatively.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07737274B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-d83951711c72435a9bf755e0eb273d0b |
| 出典メモ | uspto-grants-2010_06 |