Dimethylformamide dimethyl acetal → HCID 67280479、化合物
反応式
[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][C:10]=1[CH2:16][C:17]([CH3:19])=[O:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.CO[CH:22](OC)[N:23]([CH3:25])[CH3:24]>C1(C)C=CC=CC=1>[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][C:10]=1/[C:16](=[CH:22]/[N:23]([CH3:25])[CH3:24])/[C:17](=[O:18])[CH3:19])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1参加物
4
反応条件
- 温度
- 100 °C
実験手順
A mixture of the product from step (ii) (5.72 g) and dimethylformamide dimethyl acetal (3.5 ml) in toluene (50 ml) were heated at 100° C. for 12 h. The solvent was evaporated under reduced pressure to give an oil, 6.37 g.
後処理
- customThe solvent was evaporated under reduced pressure
- customto give an oil, 6.37 g
出典と根拠
- ORDレコード
- ord-bf319defa4164d12ad87ba081d583e13
- 出典データセット
- uspto-grants-2012_04
- 特許番号
- US08158820B2
反応ノート
読み込み中…