化工社化工社 化学情報印刷レポート · 研究参考用
(2S)-2-(2-borono-4-chlorophenoxy)-propanoic acid → [[2',5-Dichloro-4'-[(dimethylamino)sulfonyl][1,1'-biphenyl]-2-yl]oxy]-(2s)-propanoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (2S)-2-(2-borono-4-chlorophenoxy)-propanoic acid | HCID 67277298 | — |
| 反応物 | 3-Chloro-4-iodo-N,N-dimethylbenzenesulfonamide | HCID 67280204 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | [[2',5-Dichloro-4'-[(dimethylamino)sulfonyl][1,1'-biphenyl]-2-yl]oxy]-(2s)-propanoic acid | HCID 58333648 | — |
反応手順
The title compound was prepared by the method of example 144 step (i) using the product from example 151 step (iv), the product from example 148 step (ii) and methanol as solvent. Yield (0.08 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08158820B2 |
| 出典データセット | uspto-grants-2012_04 |
| ORD ID | ord-58239a4d6a9a4aecbd462b5f965d84e1 |
| 出典メモ | uspto-grants-2012_04 |