Methylamine → HCID 67274029、化合物
反応式
C(O[C:4](=[O:13])[C:5]1[CH:10]=[C:9]([NH2:11])[N:8]=[C:7]([NH2:12])[CH:6]=1)C.[CH3:14][NH2:15]>CO>[NH2:11][C:9]1[CH:10]=[C:5]([CH:6]=[C:7]([NH2:12])[N:8]=1)[C:4]([NH:15][CH3:14])=[O:13]参加物
4
反応条件
- 温度
- 70 °C
実験手順
A mixture of 0.270 g 2,6-diaminoisonicotinic acid ethyl ester and 5 ml of a 2M solution of methylamine in methanol was stirred at 70° C. for 24 h. The solvent were evaporated and the residue was triturated with ethyl acetate to yield 0.214 g of the title compound as light brown solid. MS (ISP) M+H+=167.4
後処理
- customThe solvent were evaporated
- customthe residue was triturated with ethyl acetate
出典と根拠
- ORDレコード
- ord-aea08b56640f48c29b81bec149bfe27c
- 出典データセット
- uspto-grants-2012_04
- 特許番号
- US08163778B2
反応ノート
読み込み中…