戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 1697412作成日:2026年10月27日

(2Z)-3-(2-cyanophenyl)prop-2-enoic acid → 3-(2-Cyanophenyl)propanoic acid

https://huagongshe.com/reaction/1697412

反応式

関与物質

役割名称HCID仕込み量
反応物(2Z)-3-(2-cyanophenyl)prop-2-enoic acidHCID 1899166—
反応物HCID 178418361HCID 178418361—
触媒PalladiumHCID 23938—
溶媒EthanolHCID 702—
生成物3-(2-Cyanophenyl)propanoic acidHCID 1239885090.7%

反応手順

A slurry of (Z)-3-(2-cyanophenyl)acrylic acid (Example 323a, 4.75 g) in ethanol (50 mL) was added to 5% Palladium (0.292 g) in ethanol (50 mL) and hydrogenated under 2.0 bar hydrogen pressure for 2 h. The reaction mixture was filtered and the filtrate evaporated to dryness to afford the sub title compound as a solid (4.36 g).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08163905B2
出典データセットuspto-grants-2012_04
ORD IDord-82e1327fc6404c0b893a6755157a34ae
出典メモuspto-grants-2012_04