化工社化工社 化学情報印刷レポート · 研究参考用
(Oxan-4-yl)hydrazine hydrochloride → HCID 66771862、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (Oxan-4-yl)hydrazine hydrochloride | HCID 17773358 | — |
| 反応物 | (2S,4R)-Methyl 4-(2-chloro-4-fluorophenylsulfonyl)-1-(3-oxobutanethioyl)pyrrolidine-2-carboxylate | HCID 86646870 | — |
| 生成物 | HCID 66771862 | HCID 66771862 | — |
反応手順
In analogy to the procedure described in example 192 h, (2S,4R)-methyl 4-(2-chloro-4-fluorophenylsulfonyl)-1-(3-oxobutanethioyl)pyrrolidine-2-carboxylate was reacted with (tetrahydro-pyran-4-yl)-hydrazine hydrochloride (CAS Reg. No. 116312-69-7) to give the title compound as yellow solid. MS (ESI): m/z=486.2 [M+H]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08163793B2 |
| 出典データセット | uspto-grants-2012_04 |
| ORD ID | ord-552412450de2454085430502de1bf2c1 |
| 出典メモ | uspto-grants-2012_04 |