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2-Bromo-1-(2-chloro-4-methoxyphenyl)-propan-1-one → 4-(2-Chloro-4-methoxyphenyl)-5-methyl-2-[N-(2-methoxy-5-nitrophenyl)-N-propylamino]thiazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Bromo-1-(2-chloro-4-methoxyphenyl)-propan-1-one | HCID 11054985 | — |
| 反応物 | N-(2-methoxy-5-nitrophenyl)-N-propylthiourea | HCID 18322274 | — |
| 生成物 | 4-(2-Chloro-4-methoxyphenyl)-5-methyl-2-[N-(2-methoxy-5-nitrophenyl)-N-propylamino]thiazole | HCID 18322231 | — |
反応手順
By carrying out the procedure according to EXAMPLE 12 and by using 2-bromo-1-(2-chloro-4-methoxyphenyl)propan-1-one (Compound 1-2) and N-(2-methoxy-5-nitrophenyl)-N-propylthiourea, the expected product is obtained in the form of a powder; m.p.=97° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06344470B1 |
| 出典データセット | uspto-grants-2002_02 |
| ORD ID | ord-95f350ebc1a14332bd49e1bc0e4ce37f |
| 出典メモ | uspto-grants-2002_02 |