化工社化工社 化学情報印刷レポート · 研究参考用
3,4-Diethoxybenzene-1-carbothioamide → 2-(3,4-Diethoxyphenyl)-4-(5-carboxy-2-pyrimidyl)thiazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,4-Diethoxybenzene-1-carbothioamide | HCID 7745250 | — |
| 反応物 | 5-Ethoxycarbonyl-2-(alpha-bromoacetyl)pyrimidine | HCID 18707325 | — |
| 生成物 | 2-(3,4-Diethoxyphenyl)-4-(5-carboxy-2-pyrimidyl)thiazole | HCID 18707372 | — |
反応手順
5-Ethoxycarbonyl-2-(α-bromoacetyl)pyrimidine and 3,4-diethoxythiobenzamide were subjected to the same reaction as in Example 1 and then to the same hydrolysis as in Example 147 to obtain 2-(3,4-diethoxyphenyl)-4-(5-carboxy-2-pyrimidyl)thiazole.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | USRE037556E1 |
| 出典データセット | uspto-grants-2002_02 |
| ORD ID | ord-322173e7f810483fb3da1fc9ace85f4e |
| 出典メモ | uspto-grants-2002_02 |