化工社化工社 化学情報印刷レポート · 研究参考用
Methyl 3-(2-chlorophenyl)propanoate → 3-(2-Chlorophenyl)propanoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 3-(2-chlorophenyl)propanoate | HCID 18913495 | — |
| 溶媒 | Sodium Hydroxide | HCID 14798 | — |
| 生成物 | 3-(2-Chlorophenyl)propanoic acid | HCID 95676 | — |
反応手順
Methyl 3-(2-chlorophenyl)propionate was refluxed in 10% aqueous sodium hydroxide (1 l.) for two hours and the reaction mixture was cooled, acidified and filtered. The filter cake was dissolved in hot aqueous sodium bicarbonate and filtered. The filtrate was acidified and filtered to yield 3-(2-chlorophenyl)propionic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04192888 |
| 出典データセット | uspto-grants-1980_03 |
| ORD ID | ord-50b52fd89ee74f889f0ab0f9aeecf7b9 |
| 出典メモ | uspto-grants-1980_03 |