化工社化工社 化学情報印刷レポート · 研究参考用
Diethylamine → N,N-Diethyl-2-isopropyl-5-methylcyclohexanecarboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethylamine | HCID 8021 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | p-Menthane-3-carboxylic acid | HCID 97896 | — |
| 反応物 | Cyclohexanecarbonyl chloride, 5-methyl-2-(1-methylethyl)- | HCID 13734319 | — |
| 生成物 | N,N-Diethyl-2-isopropyl-5-methylcyclohexanecarboxamide | HCID 93591 | — |
反応手順
Following the procedure of Example 5, p-menthane-3-carboxylic acid (1.84 g.) was reacted with thionyl chloride and the p-menth-3-oyl chloride then reacted with diethylamine (0.74 g.) in the presence of sodium hydroxide (0.4 g.). The product N,N-diethyl-p-menthane-3-carboxamide was recovered.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04193936 |
| 出典データセット | uspto-grants-1980_03 |
| ORD ID | ord-47b3d08fa72344cd8171f70924ce312b |
| 出典メモ | uspto-grants-1980_03 |