Ammonia → HCID 14770684、化合物
反応式
Cl[C:2]1[C:6]2[C:7]([Cl:11])=[CH:8][CH:9]=[CH:10][C:5]=2[S:4](=[O:13])(=[O:12])[N:3]=1.[NH3:14]>>[NH2:14][C:2]1[C:6]2[C:7]([Cl:11])=[CH:8][CH:9]=[CH:10][C:5]=2[S:4](=[O:13])(=[O:12])[N:3]=1参加物
3
実験手順
4.72 g of 3,4-dichlorobenzo[d]isothiazole-1,1-dioxide were added to 15 ml of 25% ammonia in 15 ml of ice water. After stirring at room temperature for two hours, the desired product was sucked off and dried; yield 4.20 g; melting-point 260° C.
出典と根拠
- ORDレコード
- ord-03808e3111054a448940e21fa1ea82e4
- 出典データセット
- uspto-grants-1983_04
- 特許番号
- US04379157
反応ノート
読み込み中…