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Water → Bupropion Hydrochloride

HRID 17019
ノート
印刷プレビュー

反応式

HRID 17019 の反応式
[C:1]([NH2:5])([CH3:4])([CH3:3])[CH3:2].[Cl:6][C:7]1[CH:8]=[C:9]([C:13](=[O:17])[CH:14](Br)[CH3:15])[CH:10]=[CH:11][CH:12]=1.O>CC(C)=O>[CH3:15][CH:14]([NH:5][C:1]([CH3:4])([CH3:3])[CH3:2])[C:13]([C:9]1[CH:10]=[CH:11][CH:12]=[C:7]([Cl:6])[CH:8]=1)=[O:17].[ClH:6]
参加物実験手順後処理出典と根拠反応ノート

参加物

5

反応物 3

HCID 962Water2 回HCID 6385Tert-Butylamine2 回HCID 4992116alpha-Bromo-3-chloropropiophenone

生成物 1

HCID 62884Bupropion Hydrochloride

試薬・触媒・溶媒 1

HCID 180Acetone溶媒2 回

実験手順

t-Butylamine was added to a solution of m-chloro-α-bromopropiophenone obtained above in acetone and water and the reaction mixture was refluxed for 2.5 hours. Acetone, water and excessive t-butylamine was evaproated at the temperature of 120° C. The concentrated solution was cooled down to room temperature and then extracted with 1500 ml of chloroform and 250 ml of water. The organic phase was dried with anhydrous sodium sulfate (30 g) and concentrated to dryness under reduced pressure. A solution of HCl in ethanol was added to the concentrated solution at room temperature and a crude product of bupropion hydrochloride was obtained after filtration. The crude product of bupropion hydrochloride was added to 2000 ml ethanol and heated to 70° C., decolorized by activated carbon (2 g) for 30 minutes and filtered. The filtrate was cooled and filtered to obtain wet product of bupropion hydrochloride. The wet product was dried in vacuum (−0.04˜−0.09 MPa, 70° C.) for 4 hours to obtain pure product. Total yield was 72% based on m-chloropropiophenone; and the HPLC's purify was ≧99.9%.

後処理

  1. temperaturethe reaction mixture was refluxed for 2.5 hours
  2. customwas evaproated at the temperature of 120° C
  3. extractionextracted with 1500 ml of chloroform and 250 ml of water
  4. dry with materialThe organic phase was dried with anhydrous sodium sulfate (30 g)
  5. concentrationconcentrated to dryness under reduced pressure
  6. additionA solution of HCl in ethanol was added to the concentrated solution at room temperature

出典と根拠

ORDレコード
ord-b8617ab280b7493fb302a5cd3f3e2cdc
出典データセット
uspto-grants-2010_06
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US07737302B2

反応ノート

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