化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → 5-(Chloromethyl)uracil
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | 5-(Hydroxymethyl)uracil | HCID 78168 | — |
| 生成物 | 5-(Chloromethyl)uracil | HCID 236125 | — |
反応手順
A solution of 1.4 g. (0.010 mole) of 5-hydroxymethyl uracil in 12.5 ml. of concentrated hydrochloric acid was prepared. A colorless precipitate (5-chloromethyl uracil) formed within two minutes and after about ten minutes the precipitate was collected by filtration, washed rapidly with ice cold water, dried and then suspended in 10 ml. of dimethylformamide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04350754 |
| 出典データセット | uspto-grants-1982_09 |
| ORD ID | ord-4dcebf16c68b4e21871e38c7da8478f6 |
| 出典メモ | uspto-grants-1982_09 |