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4-Cyclohexylphenol → Methyl alpha-(p-cyclohexylphenoxy)-alpha-[p-(alpha,alpha,alpha-trifluoro-m-tolyloxy)phenyl]acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Cyclohexylphenol | HCID 14327 | — |
| 反応物 | Methyl alpha-bromo-alpha-[p-(alpha,alpha,alpha-trifluoro-m-tolyloxy)phenyl]acetate | HCID 20392575 | — |
| 生成物 | Methyl alpha-(p-cyclohexylphenoxy)-alpha-[p-(alpha,alpha,alpha-trifluoro-m-tolyloxy)phenyl]acetate | HCID 12531889 | 68.5% |
反応手順
In a manner similar to Example 16, 7.62 g of methyl α-bromo-α-[p-(α,α,α-trifluoro-m-tolyloxy)phenyl]acetate was reacted with 4.4 g of p-cyclohexylphenol to give 6.5 g of product as an amber oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04125729 |
| 出典データセット | uspto-grants-1978_11 |
| ORD ID | ord-586301015da4425fbdafee667498b952 |
| 出典メモ | uspto-grants-1978_11 |