化工社化工社 化学情報印刷レポート · 研究参考用
Cypenamine Hydrochloride → HCID 178477936、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cypenamine Hydrochloride | HCID 21785 | — |
| 反応物 | 2-Methoxy-1-Pyrroline | HCID 353443 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | HCID 178477936 | HCID 178477936 | — |
反応手順
A slurry of 3.0 g (0.0152 mole) of powdered 2-phenylcyclopentylamine hydrochloride and 3 ml of O-methylbutyrolactim is allowed to stand at room temperature with occasional stirring for 6 days after which the material is covered with absolute ether. The solution is allowed to stand at room temperature for an additional 6 days. A precipitate forms which is collected and recrystallized from acetone-methanol and dried to give 2-[(2-phenylcyclopentyl)imino]pyrrolidine hydrochloride, M.P. 155°-158° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04126612 |
| 出典データセット | uspto-grants-1978_11 |
| ORD ID | ord-adfe97617efe42cd8953484d7d786219 |
| 出典メモ | uspto-grants-1978_11 |