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Phenyl Isothiocyanate → N-4-chlorobenzyl-N-cyclopentyl-N'-phenylthiourea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenyl Isothiocyanate | HCID 7673 | — |
| 反応物 | 4-chloro-N-cyclopentylbenzylamine | HCID 834083 | — |
| 生成物 | N-4-chlorobenzyl-N-cyclopentyl-N'-phenylthiourea | HCID 13018271 | 92.8% |
反応手順
Analogously to Example 1, 21 grams (0.1 mole) of N-4-chlorobenzyl-N-cyclopentylamine were reacted with 13.5 grams (0.1 mole) of phenylisothiocyanate. 32 grams of N-4-chlorobenzyl-N-cyclopentyl-N'-phenylthiourea were obtained. Yield: 92%, Melting point: 129°-132° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04127673 |
| 出典データセット | uspto-grants-1978_11 |
| ORD ID | ord-c45d45730c5d4b50b13b1fe0493dcdd3 |
| 出典メモ | uspto-grants-1978_11 |