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HRID 1706224作成日:2026年10月27日

Fosmidomycin → Fosmidomycin

https://huagongshe.com/reaction/1706224

反応式

関与物質

役割名称HCID仕込み量
反応物FosmidomycinHCID 572—
反応物Sodium HydroxideHCID 14798—
反応物Potassium AlumHCID 24856—
反応物SodiumHCID 5360545—
生成物FosmidomycinHCID 57274%
生成物AluminumHCID 5359268—

反応手順

To an aqueous solution (45 ml.) of potassium alum (9.17 g.) was added mono sodium salt of 3-(N-formyl-N-hydroxyamino)propylphosphonic acid (3.08 g.) with stirring, and the solution was adjusted to pH 6-7 with 10% aqueous sodium hydroxide solution and then stirred for 2 hours at ambient temperature. The precipitating materials were collected by filtration, washed twice with water (each 10 ml.) and dried to give aluminum salt of 3-(N-formyl-N-hydroxyamino)propylphosphonic acid (2.28 g.).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04206156
出典データセットuspto-grants-1980_06
ORD IDord-b587d404e39a46bf913f82d39f50caeb
出典メモuspto-grants-1980_06