HCID 20336032、化合物 → HCID 23453051、化合物
反応式
[CH2:1](OC1C=CC(Cl)=CC=1C(Cl)=O)[CH:2]=C.[CH2:15]([O:18][C:19]1[CH:41]=[CH:40][C:39]([Cl:42])=[CH:38][C:20]=1[C:21]([NH:23][CH2:24][CH2:25][C:26]1[CH:31]=[CH:30][C:29]([CH2:32][C:33]([O:35]CC)=[O:34])=[CH:28][CH:27]=1)=[O:22])[CH:16]=C.C(OC1C=CC(Cl)=CC=1C(NCCC1C=CC(CC(O)=O)=CC=1)=O)C=C>>[CH2:15]([O:18][C:19]1[CH:41]=[CH:40][C:39]([Cl:42])=[CH:38][C:20]=1[C:21]([NH:23][CH2:24][CH2:25][C:26]1[CH:27]=[CH:28][C:29]([CH2:32][C:33]([OH:35])=[O:34])=[CH:30][CH:31]=1)=[O:22])[CH2:16][CH2:1][CH3:2]参加物
4
実験手順
with 2-allyloxy-5-chlorobenzoyl chloride, via ethyl 4-[2-(2-allyloxy-5-chlorobenzamido)-ethyl]-phenylacetate, 4-[2-(2-allyloxy-5-chlorobenzamido)-ethyl]-phenylacetic acid; m.p. 104°-105° C., after recrystallization from ethyl acetate.
後処理
- customm.p. 104°-105° C., after recrystallization from ethyl acetate