Methylamine → HCID 57178653、化合物
反応式
O=[C:2]1[C:7]2[N:8]=[CH:9][S:10][C:6]=2[CH2:5][CH2:4][CH2:3]1.[CH3:11][NH2:12]>C(O)C>[CH3:11][N:12]=[C:2]1[C:7]2[N:8]=[CH:9][S:10][C:6]=2[CH2:5][CH2:4][CH2:3]1参加物
4
実験手順
6 g (0.039 mole) of the ketone obtained in step (d) are dissolved in 50 ml anhydrous ethanol and treated for 30 minutes with a gaseous methylamine stream. After evaporation to dryness, the residue is taken up into ether and filtered, to give 5.6 g (86%) of product, M.p. 233°-235° C.
後処理
- customAfter evaporation to dryness
- filtrationfiltered
出典と根拠
- ORDレコード
- ord-b61f206962e54c0791738650f81f1812
- 出典データセット
- uspto-grants-1980_06
- 特許番号
- US04208420
反応ノート
読み込み中…