1-Bromo-3-methylbutane → HCID 18963351、化合物

反応式

[C:1]([C:4]1[CH2:9][CH2:8][CH2:7][NH:6][CH:5]=1)(=[O:3])[CH3:2].Br[CH2:11][CH2:12][CH:13]([CH3:15])[CH3:14]>>[CH3:14][CH:13]([CH3:15])[CH2:12][CH2:11][N:6]1[CH2:7][CH2:8][CH2:9][C:4]([C:1]([CH3:2])=[O:3])=[CH:5]1

参加物

反応物 2

HCID 78911-Bromo-3-methylbutane

HCID 32845951-(1,4,5,6-Tetrahydropyridin-3-yl)ethanone

生成物 1

HCID 18963351HCID 18963351、化合物

実験手順

Methyl 1-(3-methylbutyl)-1,4,5,6-tetrahydro-3-pyridyl ketone was prepared from 3-acetyl-1,4,5,6-tetrahydropyridine and 1-bromo-3-methylbutane according to the procedure of Part b) of Example 1. The product distilled as a pale yellow oil (b.pt. 103°-106° C./0.1 mm Hg).

後処理

distillationThe product distilled as a pale yellow oil (b.pt. 103°-106° C./0.1 mm Hg)

出典と根拠

ORDレコード: ord-e0c95c9795544f9a938ced4f4985c55b
出典データセット: uspto-grants-1994_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05352793

反応ノート

読み込み中…

参加物