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Piperazine → 1-[2-(4-Pyridinyl)ethyl]piperazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Piperazine | HCID 4837 | — |
| 反応物 | 4-Vinylpyridine | HCID 7502 | — |
| 生成物 | 1-[2-(4-Pyridinyl)ethyl]piperazine | HCID 558685 | 40.1% |
反応手順
To a melt of piperazine (15 g, 0.17 mol) heated to 105° C. was added dropwise 4-vinylpyridine (1.25 mL, 0.012 mol). After refluxing the reaction for 5.5 hours, it was cooled to room temperature and chromatographed to provide 0.92 g of the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05354747 |
| 出典データセット | uspto-grants-1994_10 |
| ORD ID | ord-d993ab5620a446f4b33f5a57a94925a0 |
| 出典メモ | uspto-grants-1994_10 |