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HRID 1709084作成日:2026年10月26日

Chlorine → 3,3-Dichloro-1,1,1,2,2-pentafluoropropane

https://huagongshe.com/reaction/1709084

反応式

関与物質

役割名称HCID仕込み量
反応物ChlorineHCID 24526—
反応物3-Chloro-1,1,1,2,2-PentafluoropropaneHCID 67905—
生成物3,3-Dichloro-1,1,1,2,2-pentafluoropropaneHCID 61112—

反応手順

These solvents are readily prepared from commercially available materials by standard and well-known organic syntheses techniques. For example, to prepare 1,1-dichloro-2,2,3,3,3-pentafluoropropane, 2,2,3,3,3-pentafluoro-1-propanol and p-toluenesulfonate chloride are reacted together to form 2,2,3,3,3-pentafluoropropyl-p-toluenesulfonate. Then, N-methylpyrrolidone, lithium chloride, and the 2,2,3,3,3-pentafluoropropyl-p-toluenesulfonate are reacted together to form 1-chloro-2,2,3,3,3-pentafluoropropane. Chlorine and the 1-chloro-2,2,3,3,3-pentafluoropropane are then reacted together to form 1,1-dichloro-2,2,3,3,3-pentafluoropropane.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04947881
出典データセットuspto-grants-1990_08
ORD IDord-d6e311436e7443f4bb3cb297589585fa
出典メモuspto-grants-1990_08