Hydrochloric Acid → 110003-21-9

HRID 1710011ノート

反応式

HRID 1710011 の反応式
[NH2:1][CH2:2][CH2:3][C:4]([F:8])=[C:5]([F:7])[F:6].[ClH:9]>C(OCC)C>[ClH:9].[NH2:1][CH2:2][CH2:3][C:4]([F:8])=[C:5]([F:7])[F:6]

参加物

4

反応物 2

HCID 313Hydrochloric AcidHCID 152391453,4,4-Trifluoro-3-butene-1-amine

生成物 1

HCID 15239144110003-21-9

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

実験手順

A stirred solution of 0.4 gram (0.004 mole) of 4-amino-1,1,2-trifluoro-1-butene in 25 ml of diethyl ether was saturated with gaseous hydrochloric acid. The reaction mixture was concentrated under reduced pressure to give 0.4 gram of 4-amino-1,1,2-trifluoro-1-butene hydrochloride as a solid. The nmr spectrum was consistent with the proposed structure.

後処理

  1. concentrationThe reaction mixture was concentrated under reduced pressure

出典と根拠

ORDレコード
ord-703994b28af04b21b0f3112fbf7b8bc6
出典データセット
uspto-grants-1990_08
特許番号
US04952580

反応ノート

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