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Acetaldehyde → 4-[5-(3-Methoxy-phenyl)-thiazol-2-ylamino]-phenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetaldehyde | HCID 177 | — |
| 反応物 | p-Hydroxyphenylthiourea | HCID 2759331 | — |
| 反応物 | (4-Methoxy-phenyl)-[5-(4-methoxy-phenyl)thiazol-2-yl]-amine | HCID 11266955 | — |
| 溶媒 | Dichloromethane methanol | HCID 21226129 | — |
| 生成物 | 4-[5-(3-Methoxy-phenyl)-thiazol-2-ylamino]-phenol | HCID 11358448 | — |
反応手順
The title compound is prepared as described in Example 4 for (4-methoxy-phenyl)-[5-(4-methoxy-phenyl)-thiazol-2-yl]-amine but using (4-hydroxy-phenyl)-thiourea and 3-methoxy-phenyl)-acetaldehyde. Title compound: ES-MS: 312.9 [M−H]−; single peak at tR=6.81 min (System 1); Rf=0.28 (CH2Cl2/MeOH, 95/5).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07795288B2 |
| 出典データセット | uspto-grants-2010_09 |
| ORD ID | ord-095c54be9d7b487eb22ce7533448e967 |
| 出典メモ | uspto-grants-2010_09 |