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HRID 1713655作成日：2026年10月26日

{5-[4-(3-Dimethylamino-propoxy)-phenyl]-thiazol-2-yl}phenyl-amine → [4-(3-Dimethylamino-propoxy)-phenyl]-(5-thiophen-3-yl-thiazol-2-yl)-amine

https://huagongshe.com/reaction/1713655

反応式

関与物質

役割名称HCID仕込み量
反応物{5-[4-(3-Dimethylamino-propoxy)-phenyl]-thiazol-2-yl}phenyl-amineHCID 11245147—
反応物4-(5-Thiophen-3-yl-thiazol-2-yl-amino)-phenolHCID 11288835—
溶媒Dichloromethane methanolHCID 21226129—
生成物[4-(3-Dimethylamino-propoxy)-phenyl]-(5-thiophen-3-yl-thiazol-2-yl)-amineHCID 11405705—

反応手順

The title compound is prepared as described in Example 8 for {5-[4-(3-dimethylamino-propoxy)-phenyl]-thiazol-2-yl}phenyl-amine but starting from 4-(5-thiophen-3-yl-thiazol-2-yl-amino)-phenol (Example 12). Title compound: ES-MS: 360.0 [M+H]+; single peak at tR=6.16 min (System 1); Rf=0.12 (CH2Cl2/MeOH, 85/15).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07795288B2
出典データセットuspto-grants-2010_09
ORD IDord-3acdd498a2dc4dac8356a25ccf5bf1d4
出典メモuspto-grants-2010_09