Hydrochloric Acid → HCID 86594427、化合物

反応式

[CH3:1][O:2][C:3](=[O:21])[C@@H:4]([NH:13]C(OC(C)(C)C)=O)[CH2:5][CH2:6][N:7]([CH2:9][CH2:10][O:11][CH3:12])[CH3:8].[ClH:22]>>[ClH:22].[ClH:22].[CH3:1][O:2][C:3](=[O:21])[C@@H:4]([NH2:13])[CH2:5][CH2:6][N:7]([CH2:9][CH2:10][O:11][CH3:12])[CH3:8]

参加物

反応物 2

HCID 313Hydrochloric Acid

HCID 86594426HCID 86594426、化合物

生成物 1

HCID 86594427HCID 86594427、化合物

実験手順

(S)-2-tert-Butoxycarbonylamino-4-[(2-methoxyethyl)-methylamino]-butyric acid methyl ester (0.086 g, 0.28 mmol) was treated with HCl (1 mL of 4M in dioxane) and sonicated. The mixture was concentrated and dried under high vacuum to provide the product.

後処理

customsonicated
concentrationThe mixture was concentrated
customdried under high vacuum
customto provide the product

出典と根拠

ORDレコード: ord-aef2eacb093347ce8dd912a7062b2d64
出典データセット: uspto-grants-2010_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07799782B2

反応ノート

読み込み中…

参加物