関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Toluene | HCID 1140 | — |
| 反応物 | Boric Acid | HCID 7628 | — |
| 反応物 | 1,2-Hexadecanediol | HCID 98037 | — |
| 反応物 | Oleyl Alcohol | HCID 5284499 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 1,2-Hexadecanediol Oleyl Alcohol | HCID 86739633 | — |
反応手順
Approximately 54 g of oleyl alcohol, 51 g of 1,2-hexadecanediol and 100 g of toluene were reacted in a 1 liter reaction equipped as described in Example 1. The contents were heated to about 65° C. and 13 g of boric acid were added. The mixture was further heated up to 155° C. over a period of 4 hours until water evolution stopped. Approximately 11 ml. of water were collected by azeotropic distillation. The solvent was removed by vacuum distillation at 155° C. and the product was filtered at 90°-100° C. through diatomaceous earth.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04541941 |
|---|
| 出典データセット | uspto-grants-1985_09 |
|---|
| ORD ID | ord-41215c991e4f41bf9a161a9fc1497b32 |
|---|
| 出典メモ | uspto-grants-1985_09 |
|---|
