Acetyl chloride → HCID 20069224、化合物

HRID 1719848ノート

反応式

[C:1]1([CH:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[CH:15]=[CH2:16])[CH3:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C1(C(C2C=CC=CC=2)C)C=CC=CC=1.C(Cl)(=[O:33])C>>[C:1]1([CH:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[C:15](=[O:33])[CH3:16])[CH3:8])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

参加物

反応物 3

HCID 6367Acetyl chloride

HCID 119181,1-Diphenylethane

HCID 21696373HCID 21696373、化合物

生成物 1

HCID 20069224HCID 20069224、化合物

実験手順

These compounds can be prepared through various chemical synthesis methods. For example, phenyl(vinylphenyl)ethane is prepared by reacting diphenylethane with acetyl chloride in the presence of Friedel-Crafts catalyst to obtain phenyl(acetylphenyl)ethane, then it is reduced with sodium borohydride and dehydrated. Phenyl(isopropenylphenyl)ethane is prepared by reacting phenyl(formylpheny)ethane with a Grignard reagent such as methylmagnesium iodide, which is followed by dehydration.

後処理

customThese compounds can be prepared through various chemical synthesis methods

出典と根拠

ORDレコード: ord-44f53c32f85b4abb81ed640cd9a806ab
出典データセット: uspto-grants-1985_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04543207

反応ノート

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