化工社化工社 化学情報印刷レポート · 研究参考用
n-Nonylbenzene → trans-2-(4-n-Nonylbenzoyl)cyclohexane1-carboxylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | n-Nonylbenzene | HCID 14126 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 反応物 | (-)-trans-1,2-Cyclohexanedicarboxylic Anhydride | HCID 12261141 | — |
| 生成物 | trans-2-(4-n-Nonylbenzoyl)cyclohexane1-carboxylic acid | HCID 22859854 | — |
反応手順
The procedure described in Example 23 is followed using trans-1,2-cyclohexanedicarboxylic anhydride (20.0 g), 1-phenylnonane (200 ml), and anhydrous aluminum chloride (38.1 g). Work-up as described provided trans-2-(4-n-nonylbenzoyl)cyclohexane1-carboxylic acid (28.5 g, m.p. 84°-86° C).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05504244 |
| 出典データセット | uspto-grants-1996_04 |
| ORD ID | ord-176d633611e9469dac9bbefa4ba7deae |
| 出典メモ | uspto-grants-1996_04 |