化工社化工社 化学情報印刷レポート · 研究参考用
2-Bromopentane → 2-Bromo-4-methylheptane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Bromopentane | HCID 7890 | — |
| 反応物 | Phosphorus tribromide | HCID 24614 | — |
| 反応物 | 4-Methyl-2-heptanol | HCID 143345 | — |
| 生成物 | 2-Bromo-4-methylheptane | HCID 15332453 | — |
反応手順
17.50 g (0.135 mol) of 4-methylheptan-2-ol (3) was treated with PBr3 (13.48 g, 0.050 mol) as described above in the manufacture of 2-bromopentane (2). The product was purified by distillation at 165°-185° C. to yield 2-bromo-4-methylheptane (4).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05505951 |
| 出典データセット | uspto-grants-1996_04 |
| ORD ID | ord-5f328f31928f416d8c5050e18095dea3 |
| 出典メモ | uspto-grants-1996_04 |