化工社化工社 化学情報印刷レポート · 研究参考用
Ammonium Hydroxide → Thiophen-2-acetamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonium Hydroxide | HCID 14923 | — |
| 反応物 | 2-Thiopheneacetyl chloride | HCID 162362 | — |
| 生成物 | Thiophen-2-acetamide | HCID 78208 | 64% |
反応手順
To a mixture of concentrated NH4OH (100 mL) and ice was added 2-thiopheneacetyl chloride (13.0 g, 80.9 mmol). The desired compound crystallized from the reaction mixture. Recrystallization from hot water gave 2-thiopheneacetamide (8.08 g, 64% yield) as white crystals. mp 146°-147° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05506261 |
| 出典データセット | uspto-grants-1996_04 |
| ORD ID | ord-9790f435c18448d485b548d5d6086422 |
| 出典メモ | uspto-grants-1996_04 |