HCID 54035213、化合物 → L-Proline, 1-(1-oxo-4-phenylbutyl)-
反応式
C([O:8][C:9](=[O:26])[C@@H:10]1[CH2:14][CH2:13][CH2:12][N:11]1[C:15](=[O:25])[CH2:16][CH2:17][CH2:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)C1C=CC=CC=1>CO.[H][H]>[C:19]1([CH2:18][CH2:17][CH2:16][C:15]([N:11]2[CH2:12][CH2:13][CH2:14][C@H:10]2[C:9]([OH:26])=[O:8])=[O:25])[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1参加物
4
実験手順
To N-(4-phenylbutyryl)-L-proline benzyl ester (9.31 g) in 99% methanol (100 ml) was added 10% Pd--C (0.90 g), and the mixture was stirred at room temperature in hydrogen stream for 2 hours. The catalyst was filtered off with celite, and the filtrate was concentrated to give 6.26 g of N-(4-phenylbutyryl)-L-proline.
後処理
- filtrationThe catalyst was filtered off with celite
- concentrationthe filtrate was concentrated
出典と根拠
- ORDレコード
- ord-093d4f60198c4cb49e25d28aeb7c5dc6
- 出典データセット
- uspto-grants-1996_04
- 特許番号
- US05506256
反応ノート
読み込み中…