Ethanol → Ethyl sulfoacetate

HRID 1721388

反応式

HRID 1721388 の反応式
[S:1]([CH2:5][C:6]([OH:8])=[O:7])([OH:4])(=[O:3])=[O:2].[CH3:9][CH2:10]O>>[S:1]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])([OH:4])(=[O:3])=[O:2]

参加物

3

反応物 2

HCID 702EthanolHCID 31257Sulfoacetic acid

生成物 1

HCID 12216623Ethyl sulfoacetate

実験手順

Sulfoacetic acid (52 g, 371 mM) and EtOH (500 mL) were heated under reflux for 20 hours. The reaction mixture was cooled, and the excess ethanol was removed under vacuum to give ethyl sulfoacetate.

後処理

  1. temperatureunder reflux for 20 hours
  2. temperatureThe reaction mixture was cooled
  3. customthe excess ethanol was removed under vacuum

出典と根拠

ORDレコード
ord-25099fe8278a4bf3ab4105d4b60c77d8
出典データセット
uspto-grants-1996_04
特許番号
US05510379

関連ノート

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