Potassium → 2-(Hydroxyimino)-2-phenylacetonitrile
反応式
[K].[OH:2][N:3]=[C:4]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1COC1C=C(C)C=CC=1C)[C:5]#[N:6].CC1C=CC(C)=CC=1OCC1C=CC=CC=1COC1C=C(C)C=CC=1C>C1(C)C=CC=CC=1>[OH:2][N:3]=[C:4]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[C:5]#[N:6]参加物
5
実験手順
Thus, 1262.7 g of an aqueous solution containing 189.1 g (0.594 mol, 95.8% yield, E/Z=15/85) of the potassium salt of α-hydroxyimino-2-(2,5-dimethylphenoxymethyl)phenylacetonitrile was obtained. It was found that 1,2-bis(2,5-dimethylphenoxymethyl)benzene was not found in the aqueous solution, but contained at an amount of 33.7 g (0.097 mol, 96.1% recovery) in 594 g of toluene after washing.
後処理
- customwas obtained
- washafter washing
出典と根拠
- ORDレコード
- ord-ed5013acf4444532a0116e640392bd5e
- 出典データセット
- uspto-grants-1996_04
- 特許番号
- US05510506
反応ノート
読み込み中…