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Water → 4-N,N-dimethylaminophenylacetic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | 2,2'-Diazenediylbis(2-methylpropanimidamide) | HCID 1969 | — |
| 反応物 | Methyl Chloride | HCID 6327 | — |
| 反応物 | Acrylamide | HCID 6579 | — |
| 反応物 | Dimethylaminopropylacrylamide | HCID 18359659 | — |
| 生成物 | 4-N,N-dimethylaminophenylacetic acid | HCID 152203 | — |
反応手順
CH3CL/dimethylaminopropylacrylamide, quaternized with methyl chloride, and 29 g of acrylamide were added to 541 g of water with 200 mg azo-bisisobutyroamidine (AIBA) and after passage of nitrogen therethrough, the mixture was irradiated for 30 minutes by an Osram HWL 250-W lamp. The gel so obtained was dried to a residual water content of 9% and ground.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05512646 |
| 出典データセット | uspto-grants-1996_04 |
| ORD ID | ord-9d73673d2a234ac0a697386f14946bf3 |
| 出典メモ | uspto-grants-1996_04 |