1-Bromoisoquinoline → 1-Bromo-2-methylisoquinolinium tetrafluoroborate
反応式
[Br:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][N:3]=1.[F:12][B-:13]([F:16])([F:15])[F:14].[CH3:17][O+](C)C>C(Cl)Cl>[F:12][B-:13]([F:16])([F:15])[F:14].[Br:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][N+:3]=1[CH3:17]参加物
4
実験手順
The starting material was prepared by reaction of 1-bromoisoquinoline with trimethyloxonium tetrafluoroborate in CH2Cl2 to give 1-bromo-2-methylisoquinolinium tetrafluoroborate, m.p. 162°.
出典と根拠
- ORDレコード
- ord-520341b9c73e4f978c28e0686a4c29d2
- 出典データセット
- uspto-grants-1989_08
- 特許番号
- US04855420
反応ノート
読み込み中…